Thanks for your reply Tim.
Pins are PD4 and PD5 (PWM1B and PWM1A).
The example works perfectly:
void loop() {
for (unsigned long freq = 150; freq <= 15000; freq += 10){
toneAC(freq); // Play the frequency (150 Hz to 15 kHz).
delay(1); // Wait 1 ms so you can hear it.
}
Just not the volume, which is really what I'm after.