Tranfering float via SPI beween two arduinos

You are only waiting 20uS, not long for the slave to do all that work, and that's MINUS the time it takes to transmit a byte because you are waiting from the start of transmission but the slave doesn't get the interrupt until the end of transmission. It's also minus the 3-4uS interrupt latency.

I would try increasing that delay, even to 1mS just to remove that as a factor.


Rob